NMR Laboratory

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NMR Laboratory

NMR Spectroscopy Laboratory of the Jagiellonian Center of Innovation has an Avance III HD 400 MHz (Bruker) spectrometer equipped with gradient probes working in a mode of normal (BBO) and reverse (BBI) detection. Both probes allow for measurement of H spectra and spectra of other nuclei (wide-spectrum probes).

The equipment enables:

Identification of chemical substances with determination of chemical structure, often also of spatial structure and purity of compounds.
Performing measurements in the temperature range from -150 to + 150ºC,
measurement of 1D and 2D NMR spectra, including special correlation measurements:
- 1D: ¹H, ¹³C, ¹⁹F, ¹H{19F}, ¹⁹F{1H}, ³¹P, and more rarely: ¹¹B, ²⁹Si, ⁷⁷Se, ¹¹⁹Sn, solvent suppression ¹H, NOE, also DEPT at request
- 2D: COSY, DQCOSY, NOESY, ROESY, TOCSY, [H-C]HMBC, [H-C]HMBC1j, [H-C]HSQC, [H-C]HSQCTOCSY, [H-N]HMBC, [H-N]HSQC, [H-F]HOESY

We offer:

Determination and confirmation of chemical structure of organic compounds
Determination of spatial structure and isomerism of organic compounds
Confirmation of the chemical identity of samples
Analysis of dynamic processes in chemical compounds
Analysis of chemical preparation purity

Prices

Standard analysis: 1H, 13C, F, P -> price: 33 PLN net per spectrum
Analysis with guaranteed time – result within 12 hours from the moment when JCI obtained the sample* -> price: 60 PLN net per spectrum

Terms:

Guaranteed time analysis of 13C, maximum 5 samples per day, each with a minimum of 20 mg of substance for analysis
Guaranteed time analysis of 1H, maximum 20 samples per day, each with a minimum of 2 mg of substance for analysis

URGENT analysis – result within 4 hours from the moment when JCI obtained the sample* -> price: 150 PLN net per spectrum

Terms:

Guaranteed time analysis of 13C, maximum 1 sample per day, a minimum of 20 mg of substance for analysis
Guaranteed time analysis of 1H, maximum 10 samples per day, each with a minimum of 2 mg of substance for analysis
Before sending your samples for analysis, please contact the Head of the NMR Laboratory, Marek Żylewski, PhD

Note! For our regular clients, the results can be provided via FTP.

* If the sample is submitted to JCI on Friday after 12:00 noon, the result will be ready on Monday before 12:00.

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